1992 x-men: the animated series - season 2, episode 18
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Repo Man
Vindicator and Alpha Flight capture Wolverine and demand to know the secret of his Adamantium skeleton. As Vindicator runs tests on Wolverine to try and replicate his indestructible skeleton, the members of Alpha Flight realize that the experiments are going too far and fight to release him. With an enraged Wolverine freed, Vindicator and Alpha Flight are in for a fight they will never forget.